Advanced Photon Source

An Office of Science National User Facility

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Scanning Probe Microscopy of Functional Materials Applied Physics A Applied Physics Letters Advanced Functional Materials Advanced Materials Interfaces Cover JMR Vol 32 2017

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Genevieve N. Hall, Michael Stuckelberger, Tara Nietzold, Jessi Hartman, Ji-Sang Park, Jérémie Werner, Bjoern Niesen, Marvin L. Cummings, Volker Rose, Christophe Ballif, Maria K. Chan, David P. Fenning, and Mariana I. Bertoni, "The Role of Water in the Reversible Optoelectronic Degradation of Hybrid Perovskites at Low Pressure", The Journal of Physical Chemistry C 121, 25659 (2017).

Heath Kersell, Nozomi Shirato, Marvin Cummings, Hao Chang, Dean Miller, Daniel Rosenmann, Saw-Wai Hla, and Volker Rose, "Detecting element specific electrons from a single cobalt nanocluster with synchrotron x-ray scanning tunneling microscopy", Applied Physics Letters 111, 103102 (2017).

Volker Rose, Nozomi Shirato, Daniel Rosenmann and Saw-Wai Hla, "Characterizing physical, chemical, and magnetic properties at the nanoscale", SPIE Newsroom, 11 May 2017.

Michael Stuckelberger, Bradley West, Tara Nietzold, Barry Lai, Jörg M. Maser, Volker Rose and Mariana I. Bertoni, "Engineering solar cells based on correlative X-ray microscopy", Journal of Materials Research 32, 1825-1854 (2017).

Emeline Pouyet, Volker Rose, Carmen Soriano and Marc S. Walton, "Synchrotron Radiation and Neutrons in Art and Archaeology (SR2A) Conference 2016", Synchrotron Radiation News 30:1, 6-7 (2017).

Marvin Cummings, Nozomi Shirato, Heath Kersell, Hao Chang, Daniel Rosenmann, John W. Freeland, Dean Miller, Saw-Wai Hla, and Volker Rose, "Controlled Modulation of Hard and Soft X-ray Induced Tunneling Currents Utilizing Co-axial Metal-Insulator-Metal Probe Tips", Journal of Applied Physics 121, 015305 (2017).

Michael Stuckelberger, Tara Nietzold, Genevieve N. Hall, Bradley West, Jeremie Werner, Bjoern Niesen, Christophe Ballif, Volker Rose, David P. Fenning, and Mariana I. Bertoni, "Charge Collection in Hybrid Perovskite Solar Cells: Relation to the Nanoscale Elemental Distribution", IEEE Journal of Photovoltaics 7, 590-597 (2017).

Bradley M. West, Michael Stuckelberger, Harvey Guthrey, Lei Chen, Barry Lai, Jörg Maser, Volker Rose, William Shafarman, Mowafak Al-Jassim, Mariana I. Bertoni, "Grain Engineering: How Nanoscale Inhomogeneities Can Control Charge Collection in Solar Cells", Nano Energy 32, 488-493 (2017).

B. M. West, M. Stuckelberger, A. Jeffries, S. Gangam, B. Lai, B. Stripe, J. Maser, V. Rose, S. Vogt and M. I. Bertoni, "X-ray fluorescence at nanoscale resolution for multicomponent layered structures: a solar cell case study", Journal of Synchrotron Radiation 24, 288-295 (2017).


Yanqi Luo, Shany Gamliel, Sally Nijem, Sigalit Aharon, Martin Holt, Benjamin Stripe, Volker Rose, Mariana I. Bertoni, Lioz Etgar, David P. Fenning, "Spatially Heterogeneous Chlorine Incorporation in Organic-Inorganic Perovskite Solar Cells", Chemistry of Materials 28, 6536-6543 (2016).

Qinang Hu, Mohammed Aboustait, Taehwan Kima, M. Tyler Ley, Jeffrey W. Bullard, George Scherer, Jay C. Hanan, Volker Rose, Robert Winarski, Jeffrey Gelb, "Direct measurment of 3d structure, chemistry and mass density during induction period of C3S hydration", Cement and Concrete Research 89, 14-26 (2016).

Qinang Hu, Mohammed Aboustait, Taehwan Kima, M. Tyler Ley, Jay C. Hanan, Jeffrey Bullard, Robert Winarski, Volker Rose, "Direct three-dimensional observation of the microstructure and chemistry of C3S hydration", Cement and Concrete Research 88, 157-169 (2016).

Yoav Kashiv, Jotham R. Austin II, Barry Lai, Volker Rose, Stefan Vogt, and Malek El-Muayed, "Imaging trace element distributions in single organelles and subcellular features", Scientific Reports 6, 21437 (2016).

A. DiLullo, N. Shirato, M. Cummings, H. Kersell, H. Chang, D. Rosenmann, D. Miller, J. W. Freeland, S.-W. Hla, and V. Rose, "Local X-ray magnetic circular dichroism study of Fe/Cu(111) using a tunneling smart tip", (2016). Journal of Synchrotron Radiation 23, 574-578 (2016).

Hao Chang, Marvin Cummings, Nozomi Shirato, Benjamin Stripe, Daniel Rosenmann, Curt Preissner, John W. Freeland, Heath Kersell, Saw-Wai Hla, and Volker Rose, "Ultra-high vacuum compatible optical chopper system for synchrotron x-ray scanning tunneling microscopy", AIP Conf. Proc. 1696, 020001 (2016).

Bradley West; Michael Stuckelberger; Harvey Guthrey; Lei Chen; Barry Lai; Jörg Maser; Volker Rose; James J. Dynes; William Shafarman; Mowafak Al-Jassim; Mariana I. Bertoni, "Synchrotron x-ray characterization of alkali elements at grain boundaries in Cu(In, Ga)Se2 solar cells", Proceedings of the IEEE Explore: 43rd IEEE Photovoltaic Specialists Conference (PVSC), p. 31-34 (2016).

Yanqi Luo, Shany Gamliel, Sally Nijem, Sigalit Aharon, Martin Holt, Benjamin Stripe, Volker Rose, Mariana I Bertoni, Lioz Etgar, and David P Fenning, "Understanding the Distribution of Chlorine in Perovskite Solar Cells via X-ray Fluorescence Microscopy" Proceedings of the IEEE Explore: 43rd IEEE Photovoltaic Specialists Conference (PVSC), p. 802-803 (2016).

M. Stuckelberger, T. Nietzold, G. N. Hall, B. West, J. Werner, B. Niesen, C. Ballif, V. Rose, D. P. Fenning, M. I. Bertoni, "Elemental distribution and charge collection at the nanoscale on perovskite solar cells" Proceedings of the IEEE Explore: 43rd IEEE Photovoltaic Specialists Conference (PVSC), p. 1191-1196 (2016).

J. Maser, B. Lai, T. Buonassisi, Z. Cai, S. Chen, L. Finney, S.-C. Gleber, R. Harder, Ch. Jacobsen, W.J. Liu, C. Murray, C. Preissner, Ch. Roehrig, V. Rose, D. Shu, D. Vine, S. Vogt, "A Next-Generation In-Situ Nanoprobe Beamline for the Advanced Photon Source", Proceedings of SPIE 8851, 885106 (2013).

Martin Holt, Ross Harder, Robert Winarski, Volker Rose, "Nanoscale Hard X-ray Microscopy Methods for Materials Studies", Annu. Rev. Mater. Res. 43, 183 (2013).

Kangkang Wang, Daniel Rosenmann, Martin Holt, Robert Winarski, Saw-Wai Hla, and Volker Rose, "An easy-to-implement filter for separating photo-excited signals from topography in scanning tunneling microscopy", Rev. Sci. Instrum. 84, 063704 (2013).

Susan A. Bernal, John L. Provis, Volker Rose, Ruby Mejía de Gutiérrez, "High-Resolution X-ray Diffraction and Fluorescence Microscopy Characterization of Alkali-Activated Slag-Metakaolin Binders", J. Am. Ceram. Soc. 96, 1951 (2013).

Volker Rose, Kangkang Wang, TeYu Chien, Jon Hiller, Daniel Rosenmann, John W. Freeland, Curt Preissner, Saw-Wai Hla, "Synchrotron X-Ray Scanning Tunneling Microscopy: Fingerprinting Near to Far Field Transitions on Cu(111) Induced by Synchrotron Radiation", Adv. Funct. Mater. 23, 2646 (2013).

Francesca Casadio, Volker Rose, "High-resolution fluorescence mapping of impurities in historical zinc oxide pigments: hard X-ray nanoprobe applications to the paints of Pablo Picasso", Appl. Phys. A 111, 1 (2013).

J. L. Provis, A. Hajimohammadi, C.E. White, R.J. Myers, S.A. Bernal, R.P. Winarski, V. Rose, Th.E. Proffen, A. Llobet, J.S.J. van Deventer, "Nanostructural characterization of geopolymers by advanced beamline techniques", Cem. Concr. Comp. 36, 56 (2013).

R.P. Winarski, M.V. Holt, V. Rose, P. Fuesz, D. Carbaugh, C. Benson, D. Shu, D. Kline, G.B. Stephenson, I. McNulty, J. Maser, "A Hard X-ray Nanoprobe Beamline for Nanoscale Microscopy", J. Synchrotron Rad. 19, 1056 (2012).

M.I. Bertoni, G. Sarau, D.P. Fenning, D.P. Rinio, V. Rose, J. Maser, T. Buonassisi, "Nano-XRF and micro-raman studies of metal impurity decoration around dislocations in multicrystalline silicon", Proceedings of the IEEE Explore: 38th IEEE Photovoltaic Specialists Conference (PVSC), p. 1613 (2012).

J. L. Provis, R.J. Myers, C.E. White, V. Rose, J.S.J. van Deventer, "X-ray microtomography shows pore structure and tortuosity in alkali-activated binders", Cem. Concr. Res. 42, 855 (2012).

V. Rose, T.Y. Chien, J.W. Freeland, J. Hiller, D. Rosenmann, V. Metlushko, "Spin-dependent synchrotron x-ray excitations studied by scanning tunneling microscopy", J. Appl. Phys. 111, 07E304 (2012).

M.L. Cummings, TeYu Chien, C. Preissner, V. Madhavan, D. Diesing, M. Bode, J.W. Freeland, V. Rose, "Combining Scanning Tunneling Microscopy and Synchrotron Radiation for High-Resolution Imaging and Spectroscopy with Chemical, Electronic, and Magnetic Contrast", Ultramicroscopy 112, 22 (2012).

V. Rose, T.Y. Chien, J. Hiller, D. Rosenmann, R.P. Winarski, "X-ray nanotomography of SiO2-coated Pt90Ir10 tips with sub-micron conducting apex", Appl. Phys. Lett. 99, 173102 (2011).

J.L. Provis, I. Ismail, R.J. Myers, V. Rose, J.S.J. van Deventer, "Characterising the structure and permeability of alkali-activated binders", in International RILEM Conference on Advances in Construction Materials Through Science and Engineering, Ch. Leung, K.T. Wan (Eds.), RILEM Publications SARL, Pro079, pg 493-501 (2011).

M.I. Bertoni, D.P. Fenning, V. Rose, M. Holt, J. Maser, T. Buonassisi, "Synchrotron-based characterization of solar cell nanodefects", Proceedings of the IEEE Explore: 37th IEEE Photovoltaic Specialists Conference (PVSC), p. 154 (2011).

H. Yan, V. Rose, D. Shu, E. Lima, H.C. Kang, R. Conley, C. Liu, N. Jahedi, A.T. Macrander, G.B. Stephenson, M. Holt, Y.S. Chu, M. Lu, J. Maser, "Two dimensional hard x-ray nanofocusing with crossed multilayer Laue lenses", Optics Express 19, 15069 (2011).

J.P. Strachan, G. Medeiros-Ribeiro, J.J. Yang, M.-X. Zhang, F. Miao, I. Goldfarb, M. Holt, V. Rose, R.S. Williams, "Spectromicroscopy of tantalum oxide memristors", Appl. Phys. Lett. 98, 242114 (2011).

J. L. Provis, V. Rose, R. P. Winarski, J.S.J van Deventer, "Hard X-ray nanotomography of amorphous aluminosilicate cements", Scripta Materialia 65, 316 (2011).

M.I. Bertoni, D.P. Fenning, M. Rinio, V. Rose, M. Holt, J. Maser, T. Buonassisi, "Nanoprobe X-ray fluorescence characterization of defects in large-area solar cells", Energy Environ. Sci. 4, 4252 (2011).

S. A. Bernal, J. L. Provis, V. Rose, R. M. de Gutierrez, "Evolution of binder structure in sodium silicate-activated slag-metakaolin blends", Cem. Concr. Comp. 33, 46 (2011).

V. Rose, J.W. Freeland, S.K. Streiffer, "New Capabilities at the Interface of X-rays and Scanning Tunneling Microscopy", in Scanning Probe Microscopy of Functional Materials: Nanoscale Imaging and Spectroscopy, S.V. Kalinin, A. Gruverman, (Eds.), Springer, New York, pg 405-432 (2011).

V. Rose, J.W. Freeland, "A New Concept for Quantitative Nanoscale Imaging With Magnetic Contrast: Synchrotron X-ray Enhanced Scanning Tunneling Microscopy", Proceedings of the IEEE Explore: International Conference on Electromagnetics in Advanced Applications (ICEAA), p. 201 (2010)

C. Preissner, V. Rose, C. Pitts, "Mechanical Systems for a Synchrotron X-ray Enhanced Scanning Tunneling Microscope", Diamond Light Source Proc. 1, e21 (2010).

V. Rose, J.W. Freeland, "Nanoscale chemical imaging using synchrotron x-ray enhanced scanning tunneling microscopy", AIP Conf. Proc. 1234, 445 (2010).

S. A. Bernal, R. M. de Gutierrez, J. L. Provis, V. Rose, "Effect of silicate modulus and metakaolin incorporation on the carbonation of alkali silicate-activated slags", Cem. Concr. Res. 40, 898 (2010).

J.L. Provis, V. Rose, S.A. Bernal, J.S.J. van Deventer, "High resolution Nanoprobe X-ray fluorescence characterization of heterogeneous calcium and heavy metal distribution in alkali activated fly ash", Langmuir 25, 11897 (2009).

V. Rose, R. Franchy, "The band gap of ultra-thin amorphous and well-ordered Al2O3 films on CoAl(100) measured by scanning tunneling spectroscopy", J. Appl. Phys. 105, 07C902 (2009).

V. Rose, J.W. Freeland, K.E. Gray, S.K. Streiffer, "X-ray-excited photoelectron detection using a scanning tunneling microscope", Appl. Phys. Lett. 92, 193510 (2008).

S.A. Bernal, E. Rodriguez, R.M. de Gutiérrez, V. Rose, F. Puertas, S. Delvasto, "Carbonation behavior of mortar produced by alkali-activation of granular blast furnace slag", Proc. 23rd Intern. Conf. of Solid Waste Tech. & Management 23, 945-956 (2008).

V. Rose, K. Brüggemann, R. David, R. Franchy, "Oxidation induced high-Curie-temperature ferromagnetism in CoAl(100)", Phys. Stat. Sol. C 4, 4188 (2007).

V. Rose, X.M. Cheng, D.J. Keavney, J.W. Freeland, K.S. Buchanan, B. Ilic, V. Metlushko, "The breakdown of the fingerprinting of vortices by hysteresis loops in circular multilayer ring arrays", Appl. Phys. Lett. 91, 132501 (2007)

V. Podgursky, V. Rose, I. Costina, R. Franchy, "Study of phase transitions within alumina grown on top of CoAl(100) surface", Surf. Sci. 601, 3315 (2007).

R.F. Wang, J. Li, W. McConville, C. Nisoli, X. Ke, J.W. Freeland, V. Rose, M. Grimsditsch, P. Lammert, V.H. Crespi, P. Schiffer, "Demagnetization protocols for frustrated interacting nanomagnet arrays", J. Appl. Phys. 101, 09J104 (2007).

V. Rose, R. Franchy, "Thermal stability of Co-core-CoO-shell nanoparticles on an ultra-thin Θ-Al2O3 film support", J. Appl. Phys. 101, 086104 (2007).

V. Rose, V. Podgursky, R. David, R. Franchy, "Growth of Co nanoparticles on a nanostructured Θ-Al2O3 film on CoAl(100)", Surf. Sci. 601, 786 (2007).

V. Rose, K. Brüggemann, R. David, R. Franchy, "Two-Dimensional Surface Magnetism in the Bulk Paramagnetic Intermetallic Alloy CoAl(100)", Phys. Rev. Lett. 98, 037202 (2007).

V. Podgursky, V. Rose, I. Costina, R. Franchy, "Step flow observed on top of oxidized CoAl(100) surface", Appl. Surf. Sci. 253, 1796 (2006).

V. Podgursky, V. Rose, I. Costina, R. Franchy, "The coexistence of ϒ(ϒ’) and Θ alumina observed by STM and LEED on top of oxide layer grown on CoAl(100)", Appl. Surf. Sci. 252, 8394 (2006).

V. Rose, K. Buchanan, S.-H. Chung, M. Grimsditch, V. Metlushko, A. Hoffmann, V. Novosad, S.D. Bader, H. Ibach, "Frustrated magnetic vortices in a triad of permalloy rings: Magneto-optical Kerr effect, magnetic force microscopy, and micromagnetic simulations", Phys. Rev. B 73, 094442 (2006).

V. Rose, V. Podgursky, I. Costina, R. Franchy, H. Ibach, "High temperature oxidation of CoAl(100)", Surf. Sci. 577, 139 (2005).

V. Rose, V. Podgursky, I. Costina, R. Franchy, "Growth of ultra-thin amorphous Al2O3 films on CoAl(100)", Surf. Sci. 541, 128 (2003).